Information card for entry 4323510

Structure parameters

• Formula: C51 H45 Cl P2 Pd
• Calculated formula: C51 H45 Cl P2 Pd
• Title of publication: A Bidentate Bisphosphine Functioning in Intramolecular Aliphatic Metalation and as an NMR Spectroscopic Probe for the Metal Coordination Environment
• Authors of publication: William Lesueur; Euro Solari; Carlo Floriani; Angiola Chiesi-Villa; Corrado Rizzoli
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3354 - 3362
• a: 11.289 ± 0.001 Å
• b: 18.769 ± 0.002 Å
• c: 11.077 ± 0.001 Å
• α: 91.2 ± 0.01°
• β: 110.27 ± 0.01°
• γ: 105.26 ± 0.01°
• Cell volume: 2107.7 ± 0.4 ų
• Cell temperature: 25 K
• Ambient diffraction temperature: 295 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0399
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for all reflections: 0.1124
• Weighted residual factors for significantly intense reflections: 0.1025
• Goodness-of-fit parameter for all reflections: 1.021
• Goodness-of-fit parameter for significantly intense reflections: 1.021
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No