Information card for entry 4323516

Structure parameters

• Formula: C66 H132 K3 N12 O24 P7 W2
• Calculated formula: C66 H112 K3 N12 O24 P7 W2
• Title of publication: Rapid Inversion at Phosphorus in the [η4-(C6H11)3SnP7W(CO)3]2- and [(en)(CO)3W(η1,η4-P7)M(CO)3]3- Ions Where M = Cr, W
• Authors of publication: Scott Charles; Janet A. Danis; James C. Fettinger; Bryan W. Eichhorn
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3772 - 3778
• a: 14.396 ± 0.004 Å
• b: 17.543 ± 0.003 Å
• c: 20.518 ± 0.002 Å
• α: 82.419 ± 0.011°
• β: 76.83 ± 0.014°
• γ: 69.16 ± 0.015°
• Cell volume: 4708 ± 1.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1106
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for all reflections: 0.1576
• Weighted residual factors for significantly intense reflections: 0.1431
• Goodness-of-fit parameter for all reflections: 1.027
• Goodness-of-fit parameter for significantly intense reflections: 1.204
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No