Information card for entry 4323517

Structure parameters

• Formula: C57 H105 K2 N4 O15 P7 Sn W
• Calculated formula: C57 H105 K2 N4 O15 P7 Sn W
• Title of publication: Rapid Inversion at Phosphorus in the [η4-(C6H11)3SnP7W(CO)3]2- and [(en)(CO)3W(η1,η4-P7)M(CO)3]3- Ions Where M = Cr, W
• Authors of publication: Scott Charles; Janet A. Danis; James C. Fettinger; Bryan W. Eichhorn
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3772 - 3778
• a: 12.247 ± 0.002 Å
• b: 15.1909 ± 0.0014 Å
• c: 21.292 ± 0.003 Å
• α: 97.374 ± 0.01°
• β: 93.273 ± 0.013°
• γ: 111.217 ± 0.009°
• Cell volume: 3639.1 ± 0.9 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1533
• Residual factor for significantly intense reflections: 0.105
• Weighted residual factors for all reflections: 0.2269
• Weighted residual factors for significantly intense reflections: 0.2021
• Goodness-of-fit parameter for all reflections: 1.14
• Goodness-of-fit parameter for significantly intense reflections: 1.264
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No