Information card for entry 4327992

Structure parameters

• Formula: C32 H39 Cl Ge N2
• Calculated formula: C32 H39 Cl Ge N2
• Title of publication: Reactivity of Digermylenes toward Potassium Graphite: Synthesis and Characterization of Germylidenide Anions
• Authors of publication: Siew-Peng Chia; Hui-Xian Yeong; Cheuk-Wai So
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 1002 - 1010
• a: 9.0808 ± 0.0002 Å
• b: 26.5379 ± 0.0005 Å
• c: 14.0952 ± 0.0002 Å
• α: 90°
• β: 118.933 ± 0.001°
• γ: 90°
• Cell volume: 2972.78 ± 0.1 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0952
• Residual factor for significantly intense reflections: 0.0572
• Weighted residual factors for significantly intense reflections: 0.1605
• Weighted residual factors for all reflections included in the refinement: 0.184
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No