Information card for entry 4327993

Structure parameters

• Formula: C21 H24 Cl Ge N O2
• Calculated formula: C21 H24 Cl Ge N O2
• SMILES: [Ge]1(c2c3c(ccc2C(C)=[N]1c1c(C(C)C)cccc1C(C)C)OCO3)Cl
• Title of publication: Reactivity of Digermylenes toward Potassium Graphite: Synthesis and Characterization of Germylidenide Anions
• Authors of publication: Siew-Peng Chia; Hui-Xian Yeong; Cheuk-Wai So
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 1002 - 1010
• a: 14.9469 ± 0.0003 Å
• b: 15.6737 ± 0.0003 Å
• c: 18.6069 ± 0.0004 Å
• α: 90°
• β: 112.249 ± 0.001°
• γ: 90°
• Cell volume: 4034.55 ± 0.14 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0836
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.1042
• Weighted residual factors for all reflections included in the refinement: 0.1305
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No