Information card for entry 4328325

Structure parameters

• Formula: C38.5 H54 Cl I2 N8 O7.5 Rh2
• Calculated formula: C38.5 H54 Cl I2 N8 O7.5 Rh2
• Title of publication: Rhodium Complexes of a Chelating Ligand with Imidazol-2-ylidene and Pyridin-2-ylidene Donors: The Effect of C-Metalation of Nicotinamide Groups on Uptake of Hydride Ion
• Authors of publication: Alex McSkimming; Graham E. Ball; Mohan M. Bhadbhade; Stephen B. Colbran
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 2191 - 2203
• a: 15.706 ± 0.003 Å
• b: 13.5868 ± 0.0017 Å
• c: 23.595 ± 0.004 Å
• α: 90°
• β: 91.592 ± 0.004°
• γ: 90°
• Cell volume: 5033.1 ± 1.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2338
• Residual factor for significantly intense reflections: 0.0836
• Weighted residual factors for significantly intense reflections: 0.1772
• Weighted residual factors for all reflections included in the refinement: 0.2457
• Goodness-of-fit parameter for all reflections included in the refinement: 0.954
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No