Information card for entry 4328326

Structure parameters

• Formula: C17 H30 F6 I2 N4 O5 P Rh
• Calculated formula: C17 H30 F6 I2 N4 O5 P Rh
• Title of publication: Rhodium Complexes of a Chelating Ligand with Imidazol-2-ylidene and Pyridin-2-ylidene Donors: The Effect of C-Metalation of Nicotinamide Groups on Uptake of Hydride Ion
• Authors of publication: Alex McSkimming; Graham E. Ball; Mohan M. Bhadbhade; Stephen B. Colbran
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 2191 - 2203
• a: 15.3957 ± 0.0016 Å
• b: 11.599 ± 0.001 Å
• c: 17.6253 ± 0.0019 Å
• α: 90°
• β: 111.906 ± 0.003°
• γ: 90°
• Cell volume: 2920.2 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1557
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1189
• Weighted residual factors for all reflections included in the refinement: 0.1789
• Goodness-of-fit parameter for all reflections included in the refinement: 0.855
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No