Information card for entry 4328395

Structure parameters

• Common name: LGe-P(2-thienyl)2
• Formula: C37 H47 Ge N2 P S2
• Calculated formula: C37 H47 Ge N2 P S2
• Title of publication: Synthesis and Characterization of β-Diketiminate Germanium(II) Compounds
• Authors of publication: Ying Yang; Na Zhao; Yile Wu; Hongping Zhu; Herbert W. Roesky
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 2425 - 2431
• a: 10.3778 ± 0.0008 Å
• b: 15.2472 ± 0.0016 Å
• c: 22.2675 ± 0.0018 Å
• α: 90°
• β: 93.784 ± 0.008°
• γ: 90°
• Cell volume: 3515.8 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1275
• Residual factor for significantly intense reflections: 0.0732
• Weighted residual factors for significantly intense reflections: 0.0882
• Weighted residual factors for all reflections included in the refinement: 0.1005
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No