Information card for entry 4328396

Structure parameters

• Common name: LGeOtBu
• Formula: C33 H50 Ge N2 O
• Calculated formula: C33 H50 Ge N2 O
• Title of publication: Synthesis and Characterization of β-Diketiminate Germanium(II) Compounds
• Authors of publication: Ying Yang; Na Zhao; Yile Wu; Hongping Zhu; Herbert W. Roesky
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 2425 - 2431
• a: 13.341 ± 0.003 Å
• b: 16.611 ± 0.003 Å
• c: 15.085 ± 0.003 Å
• α: 90°
• β: 107.07 ± 0.03°
• γ: 90°
• Cell volume: 3195.7 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0451
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for significantly intense reflections: 0.0771
• Weighted residual factors for all reflections included in the refinement: 0.0823
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No