Information card for entry 4328743

Structure parameters

• Formula: C100 H99 B Ge Ir O5 P4 Rh
• Calculated formula: C100 H99 B Ge Ir O5 P4 Rh
• Title of publication: Germyl- and Germylene-Bridged Complexes of Rh/Ir and Subsequent Chemistry of a Bridging Germylene Group
• Authors of publication: Md Hosnay Mobarok; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 4020 - 4034
• a: 11.4112 ± 0.0012 Å
• b: 18.4332 ± 0.0019 Å
• c: 20.728 ± 0.002 Å
• α: 81.9654 ± 0.0012°
• β: 89.8087 ± 0.0012°
• γ: 89.6227 ± 0.0012°
• Cell volume: 4317.1 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.0349
• Weighted residual factors for significantly intense reflections: 0.0802
• Weighted residual factors for all reflections included in the refinement: 0.0878
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No