Information card for entry 4329725

Structure parameters

• Formula: Fe2 H121 N O136 Ru8 Te2 W18
• Calculated formula: Fe2 O131 Ru8 Te2 W18
• Title of publication: Bis[tetraruthenium(IV)]-Containing Polyoxometalates: [{RuIV4O6(H2O)9}2Sb2W20O68(OH)2]4- and [{RuIV4O6(H2O)9}2{Fe(H2O)2}2{β-TeW9O33}2H]-
• Authors of publication: Irina V. Kalinina; Natalya V. Izarova; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 7442 - 7444
• a: 12.7905 ± 0.0018 Å
• b: 14.7398 ± 0.0018 Å
• c: 15.741 ± 0.002 Å
• α: 100.136 ± 0.009°
• β: 100.385 ± 0.009°
• γ: 97.79 ± 0.008°
• Cell volume: 2830.3 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0815
• Residual factor for significantly intense reflections: 0.0495
• Weighted residual factors for significantly intense reflections: 0.1159
• Weighted residual factors for all reflections included in the refinement: 0.131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No