Information card for entry 4329726

Structure parameters

• Formula: H138 N4 O142 Ru8 Sb2 W20
• Calculated formula: O117 Ru8 Sb2 W20
• Title of publication: Bis[tetraruthenium(IV)]-Containing Polyoxometalates: [{RuIV4O6(H2O)9}2Sb2W20O68(OH)2]4- and [{RuIV4O6(H2O)9}2{Fe(H2O)2}2{β-TeW9O33}2H]-
• Authors of publication: Irina V. Kalinina; Natalya V. Izarova; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 7442 - 7444
• a: 12.8277 ± 0.0006 Å
• b: 14.7639 ± 0.0007 Å
• c: 15.579 ± 0.0007 Å
• α: 99.82 ± 0.003°
• β: 100.265 ± 0.003°
• γ: 98.563 ± 0.003°
• Cell volume: 2811.4 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0886
• Residual factor for significantly intense reflections: 0.0545
• Weighted residual factors for significantly intense reflections: 0.1414
• Weighted residual factors for all reflections included in the refinement: 0.1607
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No