Information card for entry 4332694

Structure parameters

• Formula: C65 H90 N8 Ni O2 P2 Ti2
• Calculated formula: C65 H78 N8 Ni O2 P2 Ti2
• Title of publication: Diligating Tripodal Amido-Phosphine Ligands: the Effect of a Proximal Antipodal Early Transition Metal on Phosphine Donor Ability in a Building Block for Heterometallic Complexes
• Authors of publication: Han, Hua; Elsmaili, Mona; Johnson, Samuel A.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 18
• Pages of publication: 7435 - 7445
• a: 15.417 ± 0.003 Å
• b: 15.812 ± 0.003 Å
• c: 16.336 ± 0.003 Å
• α: 111.303 ± 0.002°
• β: 109.839 ± 0.002°
• γ: 95.691 ± 0.002°
• Cell volume: 3375.7 ± 1.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1094
• Residual factor for significantly intense reflections: 0.0668
• Weighted residual factors for significantly intense reflections: 0.1506
• Weighted residual factors for all reflections included in the refinement: 0.1714
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No