Information card for entry 4332695

Structure parameters

• Formula: C63 H84 Cl N8 O P2 Rh Ta2
• Calculated formula: C62.99 H84 Cl0.99 N8 O0.99 P2 Rh Ta2
• Title of publication: Diligating Tripodal Amido-Phosphine Ligands: the Effect of a Proximal Antipodal Early Transition Metal on Phosphine Donor Ability in a Building Block for Heterometallic Complexes
• Authors of publication: Han, Hua; Elsmaili, Mona; Johnson, Samuel A.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 18
• Pages of publication: 7435 - 7445
• a: 14.2228 ± 0.0008 Å
• b: 14.2228 ± 0.0008 Å
• c: 25.594 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4483.7 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 176
• Hermann-Mauguin space group symbol: P 63/m
• Hall space group symbol: -P 6c
• Residual factor for all reflections: 0.0561
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for significantly intense reflections: 0.1181
• Weighted residual factors for all reflections included in the refinement: 0.1254
• Goodness-of-fit parameter for all reflections included in the refinement: 1.17
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No