Syntheses and structures of magnesium and zinc boraamidinates: EPR and DFT investigations of Li, Mg, Zn, B, and In complexes of the [PhB(NtBu)2].- anion radical.
Authors of publication
Chivers, Tristram; Eisler, Dana J.; Fedorchuk, Chantall; Schatte, Gabriele; Tuononen, Heikki M.; Boeré, René T
Journal of publication
Inorganic chemistry
Year of publication
2006
Journal volume
45
Journal issue
5
Pages of publication
2119 - 2131
a
11.008 ± 0.002 Å
b
17.524 ± 0.004 Å
c
21.343 ± 0.004 Å
α
111.85 ± 0.03°
β
102.36 ± 0.03°
γ
90.73 ± 0.03°
Cell volume
3713.4 ± 1.6 Å3
Cell temperature
123 ± 2 K
Ambient diffraction temperature
123 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1321
Residual factor for significantly intense reflections
0.0754
Weighted residual factors for significantly intense reflections
0.1855
Weighted residual factors for all reflections included in the refinement
0.2244
Goodness-of-fit parameter for all reflections included in the refinement
