Syntheses, crystal structures, and magneto-structural correlations of novel Cu(II) complexes containing a planar [Cu(mu-L1)]2 (HL1 = 3-(2-pyridyl)pyrazole) unit: from dinuclear to tetranuclear and then to one-dimensional compounds.
Authors of publication
Hu, Tong-Liang; Li, Jian-Rong; Liu, Chun-Sen; Shi, Xue-Song; Zhou, Jiang-Ning; Bu, Xian-He; Ribas, Joan
Journal of publication
Inorganic chemistry
Year of publication
2006
Journal volume
45
Journal issue
1
Pages of publication
162 - 173
a
8.773 ± 0.003 Å
b
10.25 ± 0.004 Å
c
11.198 ± 0.004 Å
α
74.796 ± 0.006°
β
70.617 ± 0.006°
γ
80.12 ± 0.006°
Cell volume
912.7 ± 0.6 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0838
Residual factor for significantly intense reflections
0.0498
Weighted residual factors for significantly intense reflections
0.1066
Weighted residual factors for all reflections included in the refinement
0.1204
Goodness-of-fit parameter for all reflections included in the refinement
