Syntheses, crystal structures, and magneto-structural correlations of novel Cu(II) complexes containing a planar [Cu(mu-L1)]2 (HL1 = 3-(2-pyridyl)pyrazole) unit: from dinuclear to tetranuclear and then to one-dimensional compounds.
Authors of publication
Hu, Tong-Liang; Li, Jian-Rong; Liu, Chun-Sen; Shi, Xue-Song; Zhou, Jiang-Ning; Bu, Xian-He; Ribas, Joan
Journal of publication
Inorganic chemistry
Year of publication
2006
Journal volume
45
Journal issue
1
Pages of publication
162 - 173
a
10.3984 ± 0.0015 Å
b
21.386 ± 0.003 Å
c
10.8701 ± 0.0016 Å
α
90°
β
95.392 ± 0.002°
γ
90°
Cell volume
2406.6 ± 0.6 Å3
Cell temperature
298 ± 2 K
Ambient diffraction temperature
298 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0449
Residual factor for significantly intense reflections
0.0337
Weighted residual factors for significantly intense reflections
0.0779
Weighted residual factors for all reflections included in the refinement
0.0815
Goodness-of-fit parameter for all reflections included in the refinement
