Information card for entry 4342184

Structure parameters

• Chemical name: <i>trans</i>-1,3-Di<i>tert</i>-butyl-2,4-bis(phenylethynyl) -[1,3,2,4]diazadiphosphetidine
• Formula: C24 H28 N2 P2
• Calculated formula: C24 H28 N2 P2
• SMILES: C(#Cc1ccccc1)P1N(C(C)(C)C)P(C#Cc2ccccc2)N1C(C)(C)C
• Title of publication: Construction of the First Rhodium(I) Cyclic Pentameric Structure [Rh(CO)Cl{(μ-N(t)BuP)2(C≡CPh)2}]5 Using (Phenylethynyl)cyclodiphosphazanes.
• Authors of publication: Siddiqui, Mujahuddin M.; Mague, Joel T.; Balakrishna, Maravanji S.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 4
• Pages of publication: 1200 - 1202
• a: 6.2529 ± 0.0005 Å
• b: 9.1433 ± 0.0007 Å
• c: 19.025 ± 0.0014 Å
• α: 90°
• β: 92.239 ± 0.001°
• γ: 90°
• Cell volume: 1086.87 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0415
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.099
• Weighted residual factors for all reflections included in the refinement: 0.1018
• Goodness-of-fit parameter for all reflections included in the refinement: 1.129
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No