Information card for entry 4342185

Structure parameters

• Formula: C131 H149 Cl5 N13 O5 P10 Rh5
• Calculated formula: C131 H149 Cl5 N13 O5 P10 Rh5
• Title of publication: Construction of the First Rhodium(I) Cyclic Pentameric Structure [Rh(CO)Cl{(μ-N(t)BuP)2(C≡CPh)2}]5 Using (Phenylethynyl)cyclodiphosphazanes.
• Authors of publication: Siddiqui, Mujahuddin M.; Mague, Joel T.; Balakrishna, Maravanji S.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 4
• Pages of publication: 1200 - 1202
• a: 15.812 ± 0.002 Å
• b: 21.489 ± 0.003 Å
• c: 22.68 ± 0.003 Å
• α: 75.41 ± 0.005°
• β: 88.901 ± 0.006°
• γ: 69.876 ± 0.005°
• Cell volume: 6983.2 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0724
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for significantly intense reflections: 0.1354
• Weighted residual factors for all reflections included in the refinement: 0.1565
• Goodness-of-fit parameter for all reflections included in the refinement: 1.116
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No