Information card for entry 4344679

Structure parameters

• Formula: C41 H67 I N2 O3 Sm
• Calculated formula: C41.0006 H67.0014 I N2 O3 Sm
• Title of publication: Amido Ln(II) Complexes Coordinated by Bi- and Tridentate Amidinate Ligands: Nonconventional Coordination Modes of Amidinate Ligands and Catalytic Activity in Intermolecular Hydrophosphination of Styrenes and Tolane.
• Authors of publication: Basalov, Ivan V.; Yurova, Olga S.; Cherkasov, Anton V.; Fukin, Georgy K.; Trifonov, Alexander A.
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 3
• Pages of publication: 1236 - 1244
• a: 10.5925 ± 0.0004 Å
• b: 10.7876 ± 0.0004 Å
• c: 19.3412 ± 0.0008 Å
• α: 104.302 ± 0.001°
• β: 93.954 ± 0.001°
• γ: 98.888 ± 0.001°
• Cell volume: 2102.57 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0426
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.0847
• Weighted residual factors for all reflections included in the refinement: 0.0883
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No