Information card for entry 4346963

Structure parameters

• Formula: C48 H443 Cl Cu24 Li32 N12 Na5 O323.5 P24 Sb4 W36
• Calculated formula: C48 H108 Cl Cu24 N12 Na3 O321.25 P24 Sb4 W36
• Title of publication: Heteroanionic Materials Based on Copper Clusters, Bisphosphonates, and Polyoxometalates: Magnetic Properties and Comparative Electrocatalytic NO(x) Reduction Studies.
• Authors of publication: Oms, Olivier; Yang, Shu; Salomon, William; Marrot, Jérôme; Dolbecq, Anne; Rivière, Eric; Bonnefont, Antoine; Ruhlmann, Laurent; Mialane, Pierre
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 4
• Pages of publication: 1551 - 1561
• a: 22.384 ± 0.003 Å
• b: 32.34 ± 0.004 Å
• c: 34.221 ± 0.004 Å
• α: 75.951 ± 0.004°
• β: 78.016 ± 0.005°
• γ: 78.695 ± 0.005°
• Cell volume: 23229 ± 5 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 11
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1257
• Residual factor for significantly intense reflections: 0.0918
• Weighted residual factors for significantly intense reflections: 0.2469
• Weighted residual factors for all reflections included in the refinement: 0.2679
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No