Information card for entry 7001478

Structure parameters

• Formula: C22 H24 Mo N2 O4 Si2
• Calculated formula: C22 H24 Mo N2 O4 Si2
• SMILES: [Mo]1([N]([Si](C)(C)C)=C2C(=[N]1[Si](C)(C)C)c1c3c2cccc3ccc1)(C#[O])(C#[O])(C#[O])C#[O]
• Title of publication: 1,2-Bis(imino)acenaphthene complexes of molybdenum and nickel
• Authors of publication: Fedushkin, Igor L.; Skatova, Alexandra A.; Lukoyanov, Anton N.; Khvoinova, Nalalie M.; Piskunov, Alexander V.; Nikipelov, Alexander S.; Fukin, Georgy K.; Lysenko, Konstantin A.; Irran, Elisabeth; Schumann, Herbert
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 24
• Pages of publication: 4689 - 4694
• a: 6.8006 ± 0.0002 Å
• b: 16.5995 ± 0.0003 Å
• c: 20.8751 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2356.52 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0394
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for significantly intense reflections: 0.0469
• Weighted residual factors for all reflections included in the refinement: 0.0487
• Goodness-of-fit parameter for all reflections included in the refinement: 0.969
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No