Information card for entry 7001479

Structure parameters

• Formula: C44 H52 N2 Ni
• Calculated formula: C44 H52 N2 Ni
• Title of publication: 1,2-Bis(imino)acenaphthene complexes of molybdenum and nickel
• Authors of publication: Fedushkin, Igor L.; Skatova, Alexandra A.; Lukoyanov, Anton N.; Khvoinova, Nalalie M.; Piskunov, Alexander V.; Nikipelov, Alexander S.; Fukin, Georgy K.; Lysenko, Konstantin A.; Irran, Elisabeth; Schumann, Herbert
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 24
• Pages of publication: 4689 - 4694
• a: 12.3259 ± 0.0012 Å
• b: 12.598 ± 0.0013 Å
• c: 13.4184 ± 0.0013 Å
• α: 69.714 ± 0.004°
• β: 78.287 ± 0.003°
• γ: 79.081 ± 0.004°
• Cell volume: 1897.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0402
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.0862
• Weighted residual factors for all reflections included in the refinement: 0.0901
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No