Information card for entry 7001480

Structure parameters

• Formula: C44 H48 N2 Ni P2 Si2
• Calculated formula: C44 H48 N2 Ni P2 Si2
• SMILES: [Ni]12([P](c3ccccc3)(c3ccccc3)CC[P]1(c1ccccc1)c1ccccc1)N([Si](C)(C)C)C12C(=N[Si](C)(C)C)c2c3c1cccc3ccc2
• Title of publication: 1,2-Bis(imino)acenaphthene complexes of molybdenum and nickel
• Authors of publication: Fedushkin, Igor L.; Skatova, Alexandra A.; Lukoyanov, Anton N.; Khvoinova, Nalalie M.; Piskunov, Alexander V.; Nikipelov, Alexander S.; Fukin, Georgy K.; Lysenko, Konstantin A.; Irran, Elisabeth; Schumann, Herbert
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 24
• Pages of publication: 4689 - 4694
• a: 17.7917 ± 0.0005 Å
• b: 14.5028 ± 0.0004 Å
• c: 17.577 ± 0.0005 Å
• α: 90°
• β: 118.579 ± 0.001°
• γ: 90°
• Cell volume: 3982.8 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0684
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.0956
• Weighted residual factors for all reflections included in the refinement: 0.1031
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No