Crystallography Open Database

Information card for entry 7001767

Preview

Coordinates	7001767.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51.3 H44.6 Cl2.6 Mo O4 P4 Rh2 S2
Calculated formula	C51.3 H42 Cl2.6 Mo O4 P4 Rh2 S2
Title of publication	Preparation of a bis(hydrosulfido) complex of Mo having a tetraphosphine co-ligand and its transformation into MoRh2 and MoIr2 mixed-metal sulfido clusters
Authors of publication	Iwasa, Kentaro; Seino, Hidetake; Niikura, Fumiya; Mizobe, Yasushi
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	31
Pages of publication	6134
a	41.2344 ± 0.0014 Å
b	11.9799 ± 0.0004 Å
c	21.7291 ± 0.0009 Å
α	90°
β	96.1025 ± 0.0007°
γ	90°
Cell volume	10673 ± 0.7 Å³
Cell temperature	293.1 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.0368
Weighted residual factors for all reflections included in the refinement	0.1131
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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