Information card for entry 7002303

Structure parameters

• Formula: C59 H66 N8 P2 Pb2 Si2
• Calculated formula: C59 H66 N8 P2 Pb2 Si2
• Title of publication: Synthesis and characterization of Sn(II), Pb(II) and Yb(II) complexes supported by [C(Ph2PNSiMe3){6-(2-RC5H3N)}]2− or [CH(Ph2PNSiMe3){6-(2-RC5H3N)}]− (R = 3,5-dimethyl-1-pyrazolyl or iminophosphoranyl) ligands
• Authors of publication: Chai, Zuo-Yun; Wang, Zhong-Xia
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 38
• Pages of publication: 8005 - 8012
• a: 9.908 ± 0.0009 Å
• b: 12.6483 ± 0.0012 Å
• c: 12.869 ± 0.0012 Å
• α: 98.515 ± 0.001°
• β: 107.279 ± 0.001°
• γ: 98.784 ± 0.002°
• Cell volume: 1489.6 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0333
• Residual factor for significantly intense reflections: 0.0245
• Weighted residual factors for significantly intense reflections: 0.0552
• Weighted residual factors for all reflections included in the refinement: 0.059
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No