Information card for entry 7002558

Structure parameters

• Formula: C25 H37 Cl2 N2 O2 V
• Calculated formula: C25 H37 Cl2 N2 O2 V
• SMILES: [V]1(Cl)(Cl)([O]2CCCC2)([O]2CCCC2)[N](c2c(C(C)C)cccc2C(C)C)=Cc2n1ccc2
• Title of publication: Novel vanadium(iii) complexes with bidentate N,N-chelating iminopyrrolide ligands: synthesis, characterization and catalytic behaviour of ethylene polymerization and copolymerization with 10-undecen-1-ol
• Authors of publication: Xu, Bao-Chang; Hu, Tao; Wu, Ji-Qian; Hu, Ning-Hai; Li, Yue-Sheng
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 41
• Pages of publication: 8854 - 8863
• a: 16.8743 ± 0.0011 Å
• b: 9.1538 ± 0.0006 Å
• c: 34.753 ± 0.002 Å
• α: 90°
• β: 103.205 ± 0.001°
• γ: 90°
• Cell volume: 5226.1 ± 0.6 ų
• Cell temperature: 187 ± 2 K
• Ambient diffraction temperature: 187 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1213
• Residual factor for significantly intense reflections: 0.0668
• Weighted residual factors for significantly intense reflections: 0.1296
• Weighted residual factors for all reflections included in the refinement: 0.1527
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No