Information card for entry 7002559

Structure parameters

• Formula: C23 H28 Cl2 F5 N2 O3 V
• Calculated formula: C23 H28 Cl2 F5 N2 O3 V
• SMILES: [V]1(Cl)(Cl)(n2cccc2C=[N]1c1c(F)c(F)c(F)c(F)c1F)([O]1CCCC1)[O]1CCCC1.O1CCCC1
• Title of publication: Novel vanadium(iii) complexes with bidentate N,N-chelating iminopyrrolide ligands: synthesis, characterization and catalytic behaviour of ethylene polymerization and copolymerization with 10-undecen-1-ol
• Authors of publication: Xu, Bao-Chang; Hu, Tao; Wu, Ji-Qian; Hu, Ning-Hai; Li, Yue-Sheng
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 41
• Pages of publication: 8854 - 8863
• a: 8.3619 ± 0.0012 Å
• b: 15.214 ± 0.002 Å
• c: 10.2809 ± 0.0014 Å
• α: 90°
• β: 93.629 ± 0.002°
• γ: 90°
• Cell volume: 1305.3 ± 0.3 ų
• Cell temperature: 185 ± 2 K
• Ambient diffraction temperature: 185 ± 2 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0844
• Residual factor for significantly intense reflections: 0.0592
• Weighted residual factors for significantly intense reflections: 0.126
• Weighted residual factors for all reflections included in the refinement: 0.1357
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No