Information card for entry 7002654

Structure parameters

• Common name: 1-chloro-3-triflouromethanesolfonato-2,4- bis(tris(trimethylsilyl)silyl)-cyclo-1,3-diphospha-2,4-diazane
• Chemical name: 1-chloro-3-triflouromethanesolfonato-2,4-bis[tris(trimethylsilyl)silyl]-cyclo- 1,3-diphospha-2,4-diazane
• Formula: C19 H54 Cl F3 N2 O3 P2 S Si8
• Calculated formula: C19 H54 Cl F3 N2 O3 P2 S Si8
• Title of publication: Hypersilylated cyclodiphosphadiazanes and cyclodiphosphadiazenium salts
• Authors of publication: Kuzora, René; Schulz, Axel; Villinger, Alexander; Wustrack, Ronald
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 42
• Pages of publication: 9304
• a: 18.508 ± 0.004 Å
• b: 13.008 ± 0.003 Å
• c: 18.329 ± 0.004 Å
• α: 90°
• β: 108.4 ± 0.03°
• γ: 90°
• Cell volume: 4187.1 ± 1.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0617
• Residual factor for significantly intense reflections: 0.0494
• Weighted residual factors for significantly intense reflections: 0.1306
• Weighted residual factors for all reflections included in the refinement: 0.1371
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No