Information card for entry 7002655

Structure parameters

• Common name: 1-chloro-2,4-bis(tris(trimethylsilyl)silyl)-cyclo-1,3- diphospha-2,4-diazenium tetrachlorogallate dichloromethane solvate
• Chemical name: 1-chloro-2,4-bis[tris(trimethylsilyl)silyl]-cyclo-1,3-diphospha-2,4-diazenium tetrachlorogallate dichloromethane solvate
• Formula: C19 H56 Cl7 Ga N2 P2 Si8
• Calculated formula: C19 H56 Cl7 Ga N2 P2 Si8
• Title of publication: Hypersilylated cyclodiphosphadiazanes and cyclodiphosphadiazenium salts
• Authors of publication: Kuzora, René; Schulz, Axel; Villinger, Alexander; Wustrack, Ronald
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 42
• Pages of publication: 9304
• a: 14.5675 ± 0.0016 Å
• b: 12.0572 ± 0.0016 Å
• c: 27.204 ± 0.004 Å
• α: 90°
• β: 101.975 ± 0.003°
• γ: 90°
• Cell volume: 4674.2 ± 1.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1047
• Residual factor for significantly intense reflections: 0.0861
• Weighted residual factors for significantly intense reflections: 0.2351
• Weighted residual factors for all reflections included in the refinement: 0.2467
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No