Information card for entry 7003792

Structure parameters

• Formula: C24 H55 N8 Nb
• Calculated formula: C24 H55 N8 Nb
• SMILES: [Nb]12([N](=C(N1C(C)C)N(C)C)C(C)C)([N](=C(N2C(C)C)N(C)C)C(C)C)(N(C)C)=NC(C)(C)C
• Title of publication: Mixed amido/imido/guanidinato complexes of niobium: potential precursors for MOCVD of niobium nitride thin films
• Authors of publication: Baunemann, Arne; Bekermann, Daniela; Thiede, Tobias B.; Parala, Harish; Winter, Manuela; Gemel, Christian; Fischer, Roland A.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 28
• Pages of publication: 3715 - 3722
• a: 19.7356 ± 0.0008 Å
• b: 18.2221 ± 0.0004 Å
• c: 18.3713 ± 0.0008 Å
• α: 90°
• β: 113.094 ± 0.004°
• γ: 90°
• Cell volume: 6077.3 ± 0.4 ų
• Cell temperature: 108 ± 2 K
• Ambient diffraction temperature: 108 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0604
• Residual factor for significantly intense reflections: 0.0375
• Weighted residual factors for significantly intense reflections: 0.0814
• Weighted residual factors for all reflections included in the refinement: 0.0915
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No