Information card for entry 7003793

Structure parameters

• Formula: C30 H67 N8 Nb
• Calculated formula: C30 H67 N8 Nb
• SMILES: [Nb]12(N(CC)CC)(=NC(C)(C)C)([N](=C(N1C(C)C)N(CC)CC)C(C)C)N(C(N(CC)CC)=[N]2C(C)C)C(C)C
• Title of publication: Mixed amido/imido/guanidinato complexes of niobium: potential precursors for MOCVD of niobium nitride thin films
• Authors of publication: Baunemann, Arne; Bekermann, Daniela; Thiede, Tobias B.; Parala, Harish; Winter, Manuela; Gemel, Christian; Fischer, Roland A.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 28
• Pages of publication: 3715 - 3722
• a: 11.4815 ± 0.0009 Å
• b: 18.2528 ± 0.0018 Å
• c: 34.814 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7296 ± 1.1 ų
• Cell temperature: 108 ± 2 K
• Ambient diffraction temperature: 108 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1845
• Residual factor for significantly intense reflections: 0.0964
• Weighted residual factors for significantly intense reflections: 0.1305
• Weighted residual factors for all reflections included in the refinement: 0.1584
• Goodness-of-fit parameter for all reflections included in the refinement: 1.211
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No