Synthesis and characterization of a spin crossover iron(II)-iron(III) mixed valence supramolecular pseudo-dimer exhibiting chiral recognition, hydrogen bonding, and pi-pi interactions.
Authors of publication
Brewer, Cynthia T.; Brewer, Greg; Butcher, Ray J.; Carpenter, Everett E.; Schmiedekamp, Ann M.; Viragh, Carol
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2007
Journal issue
3
Pages of publication
295 - 298
a
19.337 ± 0.003 Å
b
12.1087 ± 0.0019 Å
c
21.685 ± 0.004 Å
α
90°
β
91.105 ± 0.003°
γ
90°
Cell volume
5076.5 ± 1.5 Å3
Cell temperature
93 ± 2 K
Ambient diffraction temperature
93 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.1083
Residual factor for significantly intense reflections
0.0681
Weighted residual factors for significantly intense reflections
0.1315
Weighted residual factors for all reflections included in the refinement
0.149
Goodness-of-fit parameter for all reflections included in the refinement
