Synthesis and characterization of a spin crossover iron(II)-iron(III) mixed valence supramolecular pseudo-dimer exhibiting chiral recognition, hydrogen bonding, and pi-pi interactions.
Authors of publication
Brewer, Cynthia T.; Brewer, Greg; Butcher, Ray J.; Carpenter, Everett E.; Schmiedekamp, Ann M.; Viragh, Carol
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2007
Journal issue
3
Pages of publication
295 - 298
a
19.553 ± 0.002 Å
b
12.2348 ± 0.0014 Å
c
21.783 ± 0.003 Å
α
90°
β
90.548 ± 0.002°
γ
90°
Cell volume
5210.8 ± 1.1 Å3
Cell temperature
295 ± 2 K
Ambient diffraction temperature
295 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.1485
Residual factor for significantly intense reflections
0.0614
Weighted residual factors for significantly intense reflections
0.1162
Weighted residual factors for all reflections included in the refinement
0.1529
Goodness-of-fit parameter for all reflections included in the refinement
