Information card for entry 7006332

Structure parameters

• Formula: C21 H54 N3 Na3 Si3
• Calculated formula: C21 H54 N3 Na3 Si3
• SMILES: C[Si](C)(C)[N]1(C(C)(C)C)[Na][N](C(C)(C)C)([Si](C)(C)C)[Na][N]([Si](C)(C)C)(C(C)(C)C)[Na]1
• Title of publication: Reactions between a sodium amide Na[N(SiMe3)R1] (R1 = SiMe3, SiMe2Ph or But) and a cyanoalkane RCN (R = Ad or Bu(t)).
• Authors of publication: Avent, Anthony G.; Antolini, Floria; Hitchcock, Peter B.; Khvostov, Alexei V.; Lappert, Michael F.; Protchenko, Andrey V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 7
• Pages of publication: 919 - 927
• a: 8.6622 ± 0.0002 Å
• b: 12.3995 ± 0.0003 Å
• c: 15.4351 ± 0.0004 Å
• α: 78.751 ± 0.002°
• β: 80.164 ± 0.001°
• γ: 86.661 ± 0.001°
• Cell volume: 1601.55 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0611
• Residual factor for significantly intense reflections: 0.049
• Weighted residual factors for significantly intense reflections: 0.1345
• Weighted residual factors for all reflections included in the refinement: 0.1428
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No