Information card for entry 7006694

Structure parameters

• Formula: C40 H84 O12 Pb Ti2
• Calculated formula: C40 H84 O12 Pb Ti2
• Title of publication: Interplay between lead carboxylate and Ti or Zr isopropoxides in solution routes to perovskites: synthesis, molecular structures and reactivity of single source non-oxo Pb-Zr and Pb-Ti carboxylatoalkoxides supported by 2-ethylhexanoate ligands.
• Authors of publication: Brethon, Anne; Hubert-Pfalzgraf, Liliane G; Daran, Jean-Claude
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 1
• Pages of publication: 250 - 257
• a: 11.3722 ± 0.0006 Å
• b: 12.4435 ± 0.0006 Å
• c: 19.3035 ± 0.001 Å
• α: 91.624 ± 0.004°
• β: 96.393 ± 0.004°
• γ: 109.728 ± 0.005°
• Cell volume: 2549 ± 0.2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0637
• Residual factor for significantly intense reflections: 0.0554
• Weighted residual factors for significantly intense reflections: 0.1484
• Weighted residual factors for all reflections included in the refinement: 0.1586
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.7093 Å
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No