Information card for entry 7006695

Structure parameters

• Formula: C23 H48 O8 Pb Ti1.5
• Calculated formula: C23 H48 O8 Pb Ti1.5
• Title of publication: Interplay between lead carboxylate and Ti or Zr isopropoxides in solution routes to perovskites: synthesis, molecular structures and reactivity of single source non-oxo Pb-Zr and Pb-Ti carboxylatoalkoxides supported by 2-ethylhexanoate ligands.
• Authors of publication: Brethon, Anne; Hubert-Pfalzgraf, Liliane G; Daran, Jean-Claude
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 1
• Pages of publication: 250 - 257
• a: 21.6632 ± 0.0017 Å
• b: 14.2307 ± 0.0014 Å
• c: 22.7373 ± 0.0017 Å
• α: 90°
• β: 116.342 ± 0.008°
• γ: 90°
• Cell volume: 6281.7 ± 1 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.1156
• Weighted residual factors for all reflections included in the refinement: 0.1216
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No