Information card for entry 7006696

Structure parameters

• Formula: C54 H112 O17 Pb2 Zr2
• Calculated formula: C54 H112 O17 Pb2 Zr2
• Title of publication: Interplay between lead carboxylate and Ti or Zr isopropoxides in solution routes to perovskites: synthesis, molecular structures and reactivity of single source non-oxo Pb-Zr and Pb-Ti carboxylatoalkoxides supported by 2-ethylhexanoate ligands.
• Authors of publication: Brethon, Anne; Hubert-Pfalzgraf, Liliane G; Daran, Jean-Claude
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 1
• Pages of publication: 250 - 257
• a: 11.3776 ± 0.001 Å
• b: 13.1183 ± 0.0012 Å
• c: 26.19 ± 0.003 Å
• α: 85.559 ± 0.008°
• β: 83.667 ± 0.007°
• γ: 76.41 ± 0.008°
• Cell volume: 3771 ± 0.7 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0568
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.1165
• Weighted residual factors for all reflections included in the refinement: 0.1225
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.7093 Å
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No