Information card for entry 7006998

Structure parameters

• Formula: C36 H54 Li2 N4 O2 Si2
• Calculated formula: C36 H54 Li2 N4 O2 Si2
• SMILES: [Li]12([O](CC)CC)[N](c3ccccc3)([Si](C)(C)[NH]1c1ccccc1)[Li]1([O](CC)CC)[N]2(c3ccccc3)[Si](C)(C)[NH]1c1ccccc1
• Title of publication: A convenient route to silyl linked bis(amidinate) ligands and synthesis of group(I) metal derivatives.
• Authors of publication: Bai, Sheng-Di; Guo, Jian-Ping; Liu, Dian-Sheng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 18
• Pages of publication: 2244 - 2250
• a: 10.7863 ± 0.0017 Å
• b: 10.3647 ± 0.0016 Å
• c: 16.405 ± 0.003 Å
• α: 90°
• β: 91.373 ± 0.002°
• γ: 90°
• Cell volume: 1833.5 ± 0.5 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0591
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.1321
• Weighted residual factors for all reflections included in the refinement: 0.1364
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No