Information card for entry 7006999

Structure parameters

• Formula: C48 H66 N4 Na2 O4 Si
• Calculated formula: C48 H66 N4 Na2 O4 Si
• SMILES: [Si](/N=C([N-]c1c(cccc1C)C)\c1ccccc1)(/N=C([N-]c1c(cccc1C)C)\c1ccccc1)(C)C.[Na+].[Na+].O1CCCC1.O1CCCC1.O1CCCC1.O1CCCC1
• Title of publication: A convenient route to silyl linked bis(amidinate) ligands and synthesis of group(I) metal derivatives.
• Authors of publication: Bai, Sheng-Di; Guo, Jian-Ping; Liu, Dian-Sheng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 18
• Pages of publication: 2244 - 2250
• a: 22.975 ± 0.009 Å
• b: 21.168 ± 0.008 Å
• c: 10.86 ± 0.004 Å
• α: 90°
• β: 112.372 ± 0.005°
• γ: 90°
• Cell volume: 4884 ± 3 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0951
• Residual factor for significantly intense reflections: 0.0732
• Weighted residual factors for significantly intense reflections: 0.1824
• Weighted residual factors for all reflections included in the refinement: 0.1981
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No