Information card for entry 7007440

Structure parameters

• Chemical name: carbonylbis(1,3-bis(diphenylstibino)propane)rhodium(I) hexafluorophosphate(V) dichloromethane solvate
• Formula: C55.75 H53.5 Cl1.5 F6 O P Rh Sb4
• Calculated formula: C55.75 H53.5 Cl1.5 F6 O P Rh Sb4
• Title of publication: Synthesis and properties of Rh(I) and Ir(I) distibine complexes with organometallic co-ligands.
• Authors of publication: Brown, Michael D.; Levason, William; Reid, Gillian; Webster, Michael
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 33
• Pages of publication: 4039 - 4046
• a: 13.5141 ± 0.001 Å
• b: 20.129 ± 0.003 Å
• c: 21.133 ± 0.003 Å
• α: 74.016 ± 0.005°
• β: 80.152 ± 0.007°
• γ: 82.929 ± 0.007°
• Cell volume: 5427.5 ± 1.2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0824
• Residual factor for significantly intense reflections: 0.0509
• Weighted residual factors for significantly intense reflections: 0.0996
• Weighted residual factors for all reflections included in the refinement: 0.1109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No