Information card for entry 7007441

Structure parameters

• Chemical name: Dichloro(1,3-bis(diphenylstibino)propane)(1,3-bis(chlorophenylstibino)- propane)rhodium(III) chloride chloroform solvate
• Formula: C43 H43 Cl8 Rh Sb4
• Calculated formula: C43 H43 Cl8 Rh Sb4
• SMILES: [Rh]12([Sb](c3ccccc3)(c3ccccc3)CCC[Sb]1(c1ccccc1)c1ccccc1)([Sb]1(Cl)(c3ccccc3)CCC[Sb]2(Cl)(c2ccccc2)[Cl]1)(Cl)Cl.ClC(Cl)Cl
• Title of publication: Synthesis and properties of Rh(I) and Ir(I) distibine complexes with organometallic co-ligands.
• Authors of publication: Brown, Michael D.; Levason, William; Reid, Gillian; Webster, Michael
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 33
• Pages of publication: 4039 - 4046
• a: 28.147 ± 0.006 Å
• b: 10.9609 ± 0.0016 Å
• c: 15.724 ± 0.003 Å
• α: 90°
• β: 104.095 ± 0.008°
• γ: 90°
• Cell volume: 4705.1 ± 1.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1508
• Residual factor for significantly intense reflections: 0.1057
• Weighted residual factors for significantly intense reflections: 0.1492
• Weighted residual factors for all reflections included in the refinement: 0.173
• Goodness-of-fit parameter for all reflections included in the refinement: 1.164
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No