Information card for entry 7007695

Structure parameters

• Formula: C69 H48 Cl4 O16 P4 Pt2 Rh2 Ru5
• Calculated formula: C69 H48 Cl4 O16 P4 Pt2 Rh2 Ru5
• Title of publication: Synthesis of nonanuclear heterometallic carbide clusters. Unexpected formation of the [Ru6(CO)16]2-[Pt2(CO)2(dppm)2]2+ ion pair on the way to [Ru6C(CO)16Pt3(dppm)2].
• Authors of publication: Koshevoy, Igor O.; Haukka, Matti; Pakkanen, Tapani A.; Tunik, Sergey P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 47
• Pages of publication: 5641 - 5647
• a: 14.4758 ± 0.0002 Å
• b: 26.44 ± 0.0003 Å
• c: 19.4421 ± 0.0003 Å
• α: 90°
• β: 90.263 ± 0.003°
• γ: 90°
• Cell volume: 7441.19 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0528
• Residual factor for significantly intense reflections: 0.0381
• Weighted residual factors for significantly intense reflections: 0.0839
• Weighted residual factors for all reflections included in the refinement: 0.0887
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No