Information card for entry 7008108

Structure parameters

• Formula: C58 H55 Cl2 N5 O P3 Re
• Calculated formula: C58 H55 Cl2 N5 O P3 Re
• Title of publication: Preparation and characterization of diarylphosphazene and diarylphosphinohydrazide complexes of titanium, tungsten and ruthenium and phosphorylketimido complexes of rhenium.
• Authors of publication: Cowley, Andrew R.; Dilworth, Jonathan R.; Nairn, Alison K.; Robbie, Alasdair J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 4
• Pages of publication: 680 - 693
• a: 18.6983 ± 0.0007 Å
• b: 13.3095 ± 0.0005 Å
• c: 21.6881 ± 0.0009 Å
• α: 90°
• β: 91.669 ± 0.0016°
• γ: 90°
• Cell volume: 5395.1 ± 0.4 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0535
• Weighted residual factors for all reflections included in the refinement: 0.0583
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0666
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No