Crystallography Open Database

Information card for entry 7008109

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Structure parameters

Formula	C53.416 H48.124 Br2 N2.708 O P3 Re
Calculated formula	C53.416 H48.124 Br2 N2.708 O P3 Re
Title of publication	Preparation and characterization of diarylphosphazene and diarylphosphinohydrazide complexes of titanium, tungsten and ruthenium and phosphorylketimido complexes of rhenium.
Authors of publication	Cowley, Andrew R.; Dilworth, Jonathan R.; Nairn, Alison K.; Robbie, Alasdair J.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2005
Journal issue	4
Pages of publication	680 - 693
a	15.2069 ± 0.0002 Å
b	13.4521 ± 0.0002 Å
c	24.687 ± 0.0003 Å
α	90°
β	105.588 ± 0.0004°
γ	90°
Cell volume	4864.35 ± 0.11 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0697
Residual factor for significantly intense reflections	0.0325
Weighted residual factors for all reflections	0.0605
Weighted residual factors for significantly intense reflections	0.0352
Weighted residual factors for all reflections included in the refinement	0.0352
Goodness-of-fit parameter for all reflections included in the refinement	1.0987
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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