Information card for entry 7008514

Structure parameters

• Formula: C24 H13 Cl2 O23 Os7 Rh3
• Calculated formula: C24 H13 Cl2 O23 Os7 Rh3
• SMILES: [Os]12345([Os]678([Os]91([Rh]1%10%11%12%1326([Os]26([Os]1([Rh]1%14%15%16%102([Os]2%10([Os]1([Rh]%11%142(C9=O)C#[O])(C#[O])(C#[O])(C#[O])([H]%10)[H]%16)(C#[O])(C#[O])(C#[O])[H]%15)C#[O])(C#[O])(C#[O])(C#[O])([H]%12)[H]6)(C#[O])(C#[O])(C#[O])[H]%13)([H]4)[H]7)(C#[O])(C#[O])([H]8)[H]5)(C#[O])(C#[O])(C#[O])[H]3)(C#[O])(C#[O])C#[O].ClCCl
• Title of publication: Synthesis and structural characterization of a series of high-hydride content osmium-rhodium carbonyl complexes by the hydrogenation of arene-coordinated clusters.
• Authors of publication: Lau, Jasmine Po-Kwan; Wong, Wing-Tak
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 15
• Pages of publication: 2579 - 2587
• a: 11.792 ± 0.004 Å
• b: 24.927 ± 0.008 Å
• c: 15.438 ± 0.005 Å
• α: 90°
• β: 104.39 ± 0.01°
• γ: 90°
• Cell volume: 4395 ± 3 ų
• Cell temperature: 298 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for all reflections included in the refinement: 0.041
• Goodness-of-fit parameter for all reflections included in the refinement: 1.14
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No