Information card for entry 7009485

Structure parameters

• Formula: C30 H58 Cl2 N4 Ni2 O18
• Calculated formula: C30 H46 Cl2 N4 Ni2 O18
• Title of publication: Diversity in the reactions of unsymmetric dinucleating Schiff base ligands with CuII and NiII
• Authors of publication: Adams, Harry; Fenton, David E.; Haque, Shabana R.; Heath, Sarah L.; Ohba, Masaaki; Okawa, Hisashi; Spey, Sharon E.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 12
• Pages of publication: 1849
• a: 22.938 ± 0.006 Å
• b: 10.148 ± 0.002 Å
• c: 17.916 ± 0.004 Å
• α: 90°
• β: 111.963 ± 0.004°
• γ: 90°
• Cell volume: 3867.7 ± 1.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.2391
• Residual factor for significantly intense reflections: 0.1264
• Weighted residual factors for significantly intense reflections: 0.3124
• Weighted residual factors for all reflections included in the refinement: 0.378
• Goodness-of-fit parameter for all reflections included in the refinement: 0.991
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No