Information card for entry 7009486

Structure parameters

• Formula: C31 H58 Cl2 N4 Ni2 O17
• Calculated formula: C31 H50 Cl2 N4 Ni2 O17
• Title of publication: Diversity in the reactions of unsymmetric dinucleating Schiff base ligands with CuII and NiII
• Authors of publication: Adams, Harry; Fenton, David E.; Haque, Shabana R.; Heath, Sarah L.; Ohba, Masaaki; Okawa, Hisashi; Spey, Sharon E.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 12
• Pages of publication: 1849
• a: 10.3948 ± 0.0015 Å
• b: 10.6991 ± 0.0015 Å
• c: 10.8277 ± 0.0014 Å
• α: 73.874 ± 0.003°
• β: 85.768 ± 0.003°
• γ: 62.618 ± 0.002°
• Cell volume: 1025.2 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1126
• Residual factor for significantly intense reflections: 0.0892
• Weighted residual factors for significantly intense reflections: 0.2436
• Weighted residual factors for all reflections included in the refinement: 0.2946
• Goodness-of-fit parameter for all reflections included in the refinement: 1.202
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No