Information card for entry 7012151

Structure parameters

• Formula: C20 H17 Cl4 O P Pd
• Calculated formula: C20 H17 Cl4 O P Pd
• Title of publication: Synthesis and reactivity of bimetallic palladium(ii) methyl complexes with new functional phosphine ligands
• Authors of publication: Sub Kim, Jang; Sen, Ayusman; Guzei, Ilia A.; Liable-Sands, Louise M.; Rheingold, Arnold L.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 24
• Pages of publication: 4726
• a: 8.7474 ± 0.001 Å
• b: 9.2402 ± 0.0007 Å
• c: 13.0328 ± 0.0013 Å
• α: 94.835 ± 0.005°
• β: 90.362 ± 0.011°
• γ: 91.245 ± 0.01°
• Cell volume: 1049.38 ± 0.18 ų
• Cell temperature: 243 ± 2 K
• Ambient diffraction temperature: 243 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.036
• Residual factor for significantly intense reflections: 0.0325
• Weighted residual factors for all reflections: 0.1193
• Weighted residual factors for significantly intense reflections: 0.103
• Goodness-of-fit parameter for all reflections: 0.856
• Goodness-of-fit parameter for significantly intense reflections: 0.875
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No