Information card for entry 7012152

Structure parameters

• Formula: C24 H30 Cl O2 P Pd
• Calculated formula: C24 H30 Cl O2 P Pd
• Title of publication: Synthesis and reactivity of bimetallic palladium(ii) methyl complexes with new functional phosphine ligands
• Authors of publication: Sub Kim, Jang; Sen, Ayusman; Guzei, Ilia A.; Liable-Sands, Louise M.; Rheingold, Arnold L.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 24
• Pages of publication: 4726
• a: 10.1411 ± 0.0005 Å
• b: 11.0177 ± 0.0006 Å
• c: 12 ± 0.0006 Å
• α: 77.848 ± 0.002°
• β: 83.327 ± 0.001°
• γ: 64.925 ± 0.001°
• Cell volume: 1186.65 ± 0.11 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0571
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for all reflections: 0.1463
• Weighted residual factors for significantly intense reflections: 0.1211
• Goodness-of-fit parameter for all reflections: 1.008
• Goodness-of-fit parameter for significantly intense reflections: 0.927
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No